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filingDate 2009-02-16-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_3435a460da9913461198ead2caec092a
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publicationDate 2009-08-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber WO-2009102057-A1
titleOfInvention Successive production process for oxidized cyclic phenol sulfide
abstract Disclosed is a successive production process for an oxidized cyclic phenol sulfide represented by general formula (3), which comprises: (a first step) a step of reacting a para-alkylphenol compound (a starting material) with metal sulfur in an amount of 1.7 to 2.5 molar equivalents relative to 1 mole of the phenol compound and an alkali metal reagent in an amount of 0.25 to 0.75 molar equivalent relative to 1 mole of the phenol compound; and (a second step) a step of oxidizing a cyclic phenol sulfide represented by general formula (2) produced in the proceeding step with an oxidizing agent without removing the cyclic phenol sulfide out of a reactor, thereby producing the oxidized cyclic phenol sulfide, wherein the second step is carried out successively in the same reactor used for the first step. (In formula (2), R represents a linear or branched alkyl group having 1 to 6 carbon atoms; and m represents an integer of 4 to 8. In formula (3), R represents a linear or branched alkyl group having 1 to 6 carbon atoms; m represents an integer of 4 to 8; and n represents a number of 1 or 2.)
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