http://rdf.ncbi.nlm.nih.gov/pubchem/patent/JP-2009040630-A

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classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C30B29-12
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filingDate 2007-08-08-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_cd647d4868b051b2ec3cceb5d524b729
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publicationDate 2009-02-26-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-2009040630-A
titleOfInvention Method for producing metal fluoride single crystal using apparatus for pulling metal fluoride single crystal
abstract Provided is a method for reducing the uptake / residuality of a metal component constituting a solid scavenger, which is one factor of deterioration of internal transmittance of a metal fluoride single crystal used for an optical member or the like. To do. The scavenging reaction, the raw material melting and the crystallization are performed so that the solid scavenger used or the molten liquid thereof and the raw material metal fluoride 19 or the molten liquid 23 do not contact each other. For example, using a double structure crucible, the solid scavenger is accommodated in a member 22 having a recess provided under the opening shielding member 15 attached to the outer wall of the inner crucible 2. As a result, the raw material metal fluoride 19 accommodated in the outer crucible 1 is not in direct contact, and the gasified scavenger fills the semi-enclosed space formed by the outer crucible 1, the inner crucible 2 and the opening shielding member 15. In addition, since the residence time becomes longer, the efficiency of the scavenge reaction does not decrease. Further, even in the melting / crystallization step, it can be prevented from contacting the raw material metal fluoride melt 23. [Selection] Figure 8
priorityDate 2007-08-08-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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