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filingDate 1986-09-12-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 1987-03-26-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber WO-8701695-A2
titleOfInvention Vanillin production process
abstract In a vanillin production process, a liquid mixture containing vanillin and water is extracted with carbon dioxide at a temperature from 0o to 110oC and a pressure from 30 to 400 bar, after which the vanillin is separated. The carbon dioxide-containing vanillin is led at the extraction temperature and pressure through an aqueous solution of sulphite or hydrogen sulphite, this solution is then acidified with sulphuric acid to a pH value between 2 and 4, and the vanillin-free carbon dioxide is returned to the extraction stage.
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