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filingDate 1988-12-27-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 1990-02-06-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 1990-02-06-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-4898990-A
titleOfInvention Process for the extraction of vanillin
abstract A process for the extraction of vanillin by means of the extraction from a vanillin-containing, water-containing, liquid mixture of substances with carbon dioxide at a temperature of 0 DEG to 110 DEG C. as well as a pressure of 30 to 400 bar and a subsequent separation of vanillin is described. It is contemplated that with this process the vanillin-containing carbon dioxide is passed through an aqueous hydrogen sulfite- or sulfite-solution at the extraction temperature and the extraction pressure, that this solution is subsequently acidified with sulfuric acid to a pH value of 2 to 4, and that the vanillin-free carbon dioxide is fed back into the extraction stage.
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