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filingDate 2014-10-24-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_fe1dab52972332f15ea78405c64b45fd
publicationDate 2016-04-28-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber WO-2016064412-A1
titleOfInvention Preparation of zinc citrate and of zinc citrate-containing oral care compositions
abstract A method of preparing a zinc citrate-containing oral care composition, the method comprising: (a) adding zinc oxide to a solution of citric acid in a solvent to form a suspension; (b) agitating the suspension until a clear solution is obtained; and (c) adding an additional oral care ingredient to the solution obtained in (b). Also, a method of preparing a zinc citrate-containing oral care composition, the method comprising: (a) adding citric acid to a suspension of zinc oxide in a solvent; (b) agitating the suspension until a clear solution is obtained; and (c) adding an additional oral care ingredient to the solution obtained in (b). In both methods, steps (a) and (b) are carried out at a temperature of from 10°C to 50°C and the molar ratio of zinc oxide to citric acid in step (a) is about 3:2.
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