abstract |
Methods of more rapidly producing aerogel products by means of a rapid solvent exchange of solvent inside wet gels with supercritical CO 2 by injecting supercritical, rather than liquid, CO 2 into an extractor that has been pre-heated and pre-pressurized to substantially supercritical conditions or above. Preferably, pressure waves are applied to the supercritical CO 2 to enhance the solvent exchange. The rapid solvent exchange process is followed by depressurization, optionally with a gas exchange. Preferably, pressure waves are used to speed up the depressurization. The process greatly reduces the time for forming aerogel products. |