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filingDate 1988-01-04-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_66ddb895244676f50d3c58390a1feb60
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publicationDate 1989-07-12-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-H01175956-A
titleOfInvention Purification of optically pure 3-hydroxy acids
abstract PURPOSE: To purify an acid of short carbon chain effectively and inexpensively without using an expensive resolving agent and to obtain the title compound useful as a raw material for compounds such as agricultural chemicals in high purity, by changing a 3-hydroxy acid into a dibenzylamine salt and recrystallizing the salt in an organic solvent. n CONSTITUTION: Dibenzylamine is added to a 3-hydroxy acid having 60W85% optical purity to give dibenzylamine salt [(R*- or (S*-2]. The prepared salt is dissolved in an organic solvent such as acetonitrile or ethyl acetate, cooled and recrystallized to give optically active pure dibenzylamine salt of a (R)- or (S)-hydroxy acid. The salt is treated with an acid to give the aimed optically pure compound. n COPYRIGHT: (C)1989,JPO&Japio
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priorityDate 1988-01-04-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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Total number of triples: 36.