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filingDate 2020-12-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_c98e899db10ca7afffdb9fa378ffa662
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publicationDate 2021-05-11-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-112778170-A
titleOfInvention A kind of method and device for preparing lithium trifluoromethanesulfonate
abstract The present invention relates to a method and device for preparing lithium trifluoromethanesulfonate. The device provided by the present invention includes a raw material storage tank, a reactor, a reflux device, a gas disperser and a drying device. The method of the invention comprises: adding raw material lithium carbonate and organic solvent butanone into a reactor, after controlling the reflux temperature and the temperature of the reactor, adding trifluoromethanesulfonyl chloride from the bottom of the reactor into the reactor, and vaporizing the trifluoromethanesulfonyl chloride After passing through the gas disperser, it reacts with lithium carbonate, the carbon dioxide generated by the reaction is discharged, and the generated lithium trifluoromethanesulfonyl solution is filtered and then enters a drying device, and after drying, a lithium trifluoromethanesulfonate product is obtained. The invention has simple process, few required equipment, easy operation and high safety, effectively improves the purity of the product, and can meet the high-purity requirements of the lithium battery industry.
priorityDate 2020-12-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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