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filingDate 2020-10-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2022-07-01-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2022-07-01-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-112266620-B
titleOfInvention Silk-carbon nanotube composite material with oriented through pore channels and preparation method thereof
abstract A silk-carbon nanotube composite material with directional through pore channels is composed of carbon nanotubes and silk fibroin according to a mass ratio of 1: 20-200. Cleaning and cutting dried silkworm cocoon, adding into Na 2 CO 3 Boiling in the solution to remove the gum, cleaning, naturally drying, and dissolving in CaCl 2 -formic acid solution to obtain a fibroin solution; then adding multi-wall carbon nano tubes into the solution, dispersing at a high speed and performing ultrasonic treatment to obtain silk-carbon nano tube dispersion liquid; freezing at low temperature for 6-8h after directional freezing, then freeze-drying, soaking in water for 1-3 days, and freeze-drying again to obtain. The method is simple and quick to operate, and shortens the dissolving time; the obtained material has the oriented through pore canals with regular arrangement, high mechanical strength and good biocompatibility, and can be used as a biomedical specific tissue repair material.
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