http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-109517019-B

Outgoing Links

Predicate Object
classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07J1-0011
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07J1-00
filingDate 2017-09-18-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2021-12-07-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2021-12-07-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-109517019-B
titleOfInvention Recycling method of 3 beta-acetoxyandrostane-5-alkene-17-ketone addition reaction byproduct
abstract The invention discloses a method for preparing 3 beta-acetoxyl-5 alpha-chlorine-6 beta-hydroxyandrost-17-ketone by using solid waste 3 beta-acetoxyl-6 alpha-chlorine-5 beta-hydroxyandrost-17-ketone in the addition reaction process of 3 beta-acetoxyl androst-5 alpha-chlorine-6 beta-hydroxyandrost-17-ketone as a raw material and preparing the 3 beta-acetoxyl-5 alpha-chlorine-6 beta-hydroxyandrost-17-ketone through two-step reactions of eliminating cyclization and addition ring opening. The method can effectively recycle the by-product in the preparation process of the 3 beta-acetoxyl-5 alpha-chlorine-6 beta-hydroxyandrostan-17-ketone, is environment-friendly and reduces the production cost. The method for preparing the 3 beta-acetoxyl-5 alpha-chlorine-6 beta-hydroxyandrost-17-ketone has the advantages of simple and convenient operation, mild reaction condition and high yield.
priorityDate 2017-09-18-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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