http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-102977264-B
Outgoing Links
Predicate | Object |
---|---|
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C12P19-02 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08J3-075 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08F218-14 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08F2-24 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08F220-54 |
filingDate | 2012-11-30-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2015-08-12-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2015-08-12-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-102977264-B |
titleOfInvention | A kind of preparation method of sugary temperature-responsive microgel |
abstract | The present invention relates to a kind of preparation method of sugary temperature-responsive microgel, comprising: aliphatic diacid mixes with vinyl acetate by (1), adds catalyzer, be obtained by reacting aliphatic diacid divinyl ester in 60 ~ 75 DEG C; (2) aliphatic diacid divinyl ester and glucose are dissolved in organic solvent, then add bacillus alkaline protease or lipase LipaseAY30, the sugary hydrophilic monomer of synthesis polymerizable; (3) sugary for above-mentioned polymerizable hydrophilic monomer, NIPA monomer, linking agent, emulsifying agent is completely soluble in water; (4) by above-mentioned solution thermal-stable, pass into nitrogen deoxygenation simultaneously, add initiator, under nitrogen protection, stir, reaction, dialysis, obtains sugary temperature-responsive microgel.The inventive method synthetic route is succinct, and technical process is short, and reaction conditions is gentle, and toxicity is low, is easy to industrialization, reduce further cost; Polymerization single polymerization monomer abundance, cheap, cost is lower. |
priorityDate | 2012-11-30-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 113.