http://rdf.ncbi.nlm.nih.gov/pubchem/patent/YU-45806-B

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assignee http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_6963410cbb03c6b79d727ad6b97989a4
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D233-72
filingDate 1986-11-28-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_9d6dffe3a3d910d401e76b8d6dab27a3
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_fee3fc72097a24896f44934eec1f3e6f
publicationDate 1992-07-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber YU-45806-B
titleOfInvention PROCEDURE FOR PREPARATION OF 5-SUBSTITUTED DERIVATIVES OF 5- (3'4 ', 5', -TRIMETHOXYBENZYL) -HYDANTOIN
abstract A process for the preparation of 5-SUBSTITUTED DERIVATIVES OF 5- (3'4 ', 5', -TRIMETHOXYBENZYL) -HYDANTOIN, of general formula I, in which R has the meaning of a methyl, ethyl, n-propyl, n-butyl or allyl radical, that the 2-substituted 2- (3 ', 4', 5'-trimethoxybenzyl) -malondiamide derivatives of general formula II, in which R has the above meaning, are dissolved in a solution of sodium hypochlorite and sodium hydroxide, the resulting reaction mixture is heated to 3-5 hours at 50-70 C, then cooled to room temperature, the pH was adjusted to 6-7 by the addition of dilute hydrochloric acid, the precipitated crystals were filtered off with suction and recrystallized from alcohol, ethanol or isopropanol.
priorityDate 1986-11-28-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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