http://rdf.ncbi.nlm.nih.gov/pubchem/patent/WO-9920586-A1

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http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C29-86
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C29-16
filingDate 1998-09-29-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_28c6061b19e978d09d87496c38114f3d
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publicationDate 1999-04-29-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber WO-9920586-A1
titleOfInvention Process improvement to produce low color trimethylolpropane
abstract Disclosed is a process for acquiring crude trimethylolpropane (TMP) of low reacted color. TMP is generally prepared by the condensation of n-butyraldehyde and formaldehyde in an alkali solution. The mixture is then concentrated and placed through an extractor. It has been found that a high concentration of low color TMP is present in the extractor and may be obtained by taking a slip stream of hot organic/water/TMP from the extractor and allowing the mixture to cool and phase separate. Upon separation of the phases, TMP generally having an acid wash color of about or less than 5 GU is recovered from the water phase. Disclosed is use of a single and multistage extractor.
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priorityDate 1997-10-16-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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