Predicate |
Object |
assignee |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_d648658dd620f548c24de39659a5e9e3 |
classificationCPCInventive |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C231-02 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C303-38 |
classificationIPCAdditional |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C311-18 |
classificationIPCInventive |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C231-02 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C311-08 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C233-43 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C235-16 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C233-80 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C311-46 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C311-21 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C303-38 |
filingDate |
1997-01-29-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_5f933ab6133aaacaf0e7bacbaef7bb15 |
publicationDate |
1997-07-31-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber |
WO-9727171-A1 |
titleOfInvention |
Process for preparing n-(3-amino-4-chlorophenyl) acylamides |
abstract |
The present invention provides a process for preparing N-(3-amino-4-chlorophenyl) acylamides of Formula (I): comprising reacting, in a solvent comprising at least one polar solvent, in the presence of at least one acid acceptor, 1-chloro-2,4-diaminobenzene with at least one acyl chloride of formula (II): Cl-X-R wherein X is -CO- or -SO2-; R is selected from the group C1-C25 alkyl; C1-C25 alkyl substituted with one or more groups selected from C1-C12 alkoxy, aryl, aryloxy and C5-C7 cycloalkyl; aryl; C5-C7 cycloalkyl. The present invention further comprises the step of purifying said N-(3-amino-4-chlorophenyl) acylamides by crystallizing from a non-polar solvent or conducting the reaction in a mixture of at least one polar and at least one non-polar solvent. |
isCitedBy |
http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-111757870-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/WO-2019141230-A1 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/WO-9935122-A1 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/IL-276088-B1 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/IL-276088-B2 |
priorityDate |
1996-01-29-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type |
http://data.epo.org/linked-data/def/patent/Publication |