Predicate |
Object |
assignee |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_5c24684033fba97d1ad845ce453a57e3 |
classificationCPCInventive |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C317-28 |
classificationIPCInventive |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C315-02 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C317-28 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07B61-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/B01J23-22 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/B01J23-30 |
filingDate |
1991-02-27-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_a91fd6a14ab42ed22a65eb84bf1fefd7 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_cd9c2a2154c4e0e7e05f8edc432176b4 |
publicationDate |
1991-09-19-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber |
WO-9113866-A1 |
titleOfInvention |
Method for preparing 3'-aminopropyl-2-sulphatoethylsulphone |
abstract |
In a method for preparing 3'-aminopropyl-2-sulphatoethylsulphone in a one-pot process, allyl amine is reacted with mercaptoethanol in dilute sulphuric acid at temperatures of approximately 50 °C up to the boiling point in the presence of a radical starter. The resultant reaction mixture is oxidized with hydrogen peroxide, in the presence of catalytic quantities of a compound of a transition metal of the periodic system of the elements as an oxidation catalyst, at temperatures of approximately 70 to 100 °C and evaporated to dryness after addition of sufficient sulphuric acid to bring the total sulphuric acid content of the mixture to at least 1 mol, referred to the quantity of allyl amine used. |
isCitedBy |
http://rdf.ncbi.nlm.nih.gov/pubchem/patent/EP-0652262-A1 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/DE-19543276-C1 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/EP-0518321-A1 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-6376656-B1 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-1037839-C http://rdf.ncbi.nlm.nih.gov/pubchem/patent/EP-0639562-A1 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-6025478-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-5227527-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/WO-9215559-A1 |
priorityDate |
1990-03-07-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type |
http://data.epo.org/linked-data/def/patent/Publication |