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filingDate 1991-02-27-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_a91fd6a14ab42ed22a65eb84bf1fefd7
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publicationDate 1991-09-19-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber WO-9113866-A1
titleOfInvention Method for preparing 3'-aminopropyl-2-sulphatoethylsulphone
abstract In a method for preparing 3'-aminopropyl-2-sulphatoethylsulphone in a one-pot process, allyl amine is reacted with mercaptoethanol in dilute sulphuric acid at temperatures of approximately 50 °C up to the boiling point in the presence of a radical starter. The resultant reaction mixture is oxidized with hydrogen peroxide, in the presence of catalytic quantities of a compound of a transition metal of the periodic system of the elements as an oxidation catalyst, at temperatures of approximately 70 to 100 °C and evaporated to dryness after addition of sufficient sulphuric acid to bring the total sulphuric acid content of the mixture to at least 1 mol, referred to the quantity of allyl amine used.
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priorityDate 1990-03-07-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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