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publicationDate 2022-09-22-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber WO-2022197668-A1
titleOfInvention Systems and methods for the synthesizing zsm-22 zeolites
abstract According to one or more embodiments, non-agglomerated, nano-sized ZSM-22 zeolites may be synthesized by methods comprising operating a mechanical rotation drum unit at a first temperature of from 40°C to 60°C and a first speed of from 200 rpm to 1000 rpm for a first time period of from 1.3 hours to 2.7 hours; operating the mechanical rotation drum unit at a second speed of from 30 rpm to 90 rpm for a second time period of from 0.05 hours to 0.4 hours; heating the mechanical rotation drum unit at a ramping temperature of from 8°C/minute to 12°C/minute to a second temperature of from 115°C to 185°C at the second speed; operating the mechanical rotation drum unit at the second temperature and the second speed for a third time period of from 30 hours to 90 hours; and cooling the mechanical rotation drum unit at a fourth speed of 0 rpm.
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