http://rdf.ncbi.nlm.nih.gov/pubchem/patent/WO-2019132663-A1
Outgoing Links
Predicate | Object |
---|---|
assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_48de1cfdc993735cdc1c82f96827b33e |
classificationCPCAdditional | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07B2200-13 |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D307-68 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D307-68 |
filingDate | 2018-12-31-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_695329ce20f569e0c1c673ee14bf5c58 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_86fb8e5315494509bd63553ed5c742e5 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_2afa2105d71be2d35263761391df06e0 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_77a4679edf98d08438ef90e85fc37e91 |
publicationDate | 2019-07-04-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | WO-2019132663-A1 |
titleOfInvention | Method for purifying and removing color of fdca |
abstract | The invention is based on the finding that when conducting crystallization of FDCA at high temperatures, the formation of significant amounts of colored byproduct can be reduced or even avoided when the FDCA mixture is kept at temperatures above 100 °C for less than 15 minutes. This is achieved by conducting the crystallization process in a continuous reactor. Accordingly, the method comprises the steps of feeding a mixture comprising undissolved FDCA and a solvent to a reactor; and dissolving FDCA by superheating the mixture in the reactor to a temperature of at least 130 °C; and crystallizing FDCA by cooling the mixture in the reactor, wherein the reactor is a continuous reactor and the residence time in the reactor zone wherein the FDCA mixture has a temperature above 100 °C is less than 15 minutes. |
isCitedBy | http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-112174917-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-112174917-B http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-10882836-B1 |
priorityDate | 2017-12-29-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 31.