http://rdf.ncbi.nlm.nih.gov/pubchem/patent/WO-2019052738-A1

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filingDate 2018-07-31-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_d059e3973b676ed15ade17d66cfab462
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publicationDate 2019-03-21-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber WO-2019052738-A1
titleOfInvention PROCESS FOR PRODUCING HUMINES FROM BIOMASS SUCH AS WOOD, BARK, CEREAL STRAW, LEAVES, HERBACEOUS PLANTS AND POLYPORTS, PURIFICATION SLUDGE AND OTHER ORGANIC WASTE
abstract The invention relates to a process for the chemical synthesis of humic substances from biomass, the process comprising the following. The invention relates to a process for the chemical synthesis of humic substances from biomass, the process comprising the following process steps. First, we conduct a Maillard reaction by heating the first biomass, especially for 1 to 30 minutes, more specifically for 10 to 15 minutes, and more preferably 150-250 ° C, more preferably 160-220 ° C, more preferably 170-190 ° C, heated. The resulting soluble impurities are extracted by means of water from the obtained second biomass. The remaining first solid is torrifiziert under a protective gas atmosphere at 180-300 ° C, in particular at 190-250 ° C, in particular torrifiziert for 0.2 to 4 hours, in particular for 1.5 to 2.5 hours. An obtained torrified second solid is heated with a solution of a strong inorganic acid in excess to 120-180 ° C, in particular to 110-170 ° C, in particular 130-165 ° C, in particular for 0.5 to 3 hours, in particular for Heated for 1.5 to 2.5 hours. The resulting first reaction mixture is filtered and washed with water.
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