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publicationNumber WO-2016023112-A1
titleOfInvention System and method for metallic isotope separation by a combined thermal-vacuum distillation process
abstract A process for the separation of 99m Tc from molybdenum targets is described. The method for separation of 99m Tc isotope from molybdenum targets includes: i) providing an initial multicomponent mixture of elements, the mixture containing 99m Tc; ii) dissolving the multicomponent mixture of elements with an oxidizing agent to oxidize the mixture of elements; iii) heating the mixture of elements at a temperature sufficiently high enough to sublimate a vaporized compound containing 99m Tc; iv) condensing the vaporized compound containing 99m Tc to form a reaction product; v) adding a base to the condensed reaction product to dissolve the 99m Tc containing reaction product to form sodium pertechnetate (Na 99m TcO 4 ); and vii) purifying the crude solution of sodium pertechnetate Na 99m Tc04 using column chromatography to provide the 99m Tc isotope as a radiochemical compound.
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