http://rdf.ncbi.nlm.nih.gov/pubchem/patent/WO-2015177483-A1
Outgoing Links
| Predicate | Object |
|---|---|
| assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_37b36726b8c2d3a2fe627ab8caf1e052 http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_37f4922dfb7777b019e504b885211b8e http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_2fcd93a336b3486d9e6daeb89e4d7448 |
| classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07F5-022 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C01B6-13 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C01B35-14 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C01B35-146 |
| classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C01B35-14 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07F5-02 |
| filingDate | 2015-05-22-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_bd4edd508368afe80d96136264c659a2 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_68df65165655e790b35d97ccdb5a5c67 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_89dfe2c0cd001ab9ebd90ff583d5426c |
| publicationDate | 2015-11-26-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationNumber | WO-2015177483-A1 |
| titleOfInvention | Method for producing borazane |
| abstract | The present invention relates to a method for producing borazane (NH 3 -BH 3 ). The method includes: providing a reactor (1), provided with stirring means and a thermostat set to a temperature of θ 1 to 40 °C; injecting anhydrous liquid ammonia (NH 3 (l)) into said reactor (1); injecting a borane-amine complex (Am.BH 3 ) into said reactor (1) containing the anhydrous liquid ammonia (NH 3 (l)) while stirring, wherein said borane-amine complex (Am.BH 3 ), the corresponding amine (Am) of which is only soluble in anhydrous liquid ammonia at a rate of less than 10 g in 100 g of ammonia at 20 °C, is injected in an amount such that the molar ratio R = anhydrous liquid ammonia (NH 3 (l)) / borane-amine complex (Am.BH 3 ) is no lower than 5; stirring the mixture; halting the stirring and obtaining, within said reactor (1), two demixed phases: a light phase (1a) made up essentially of an anhydrous liquid ammonia solution (NH 3 (l)) containing borazane, and a heavy phase (1b) made up essentially of the amine (Am) corresponding to the injected borane-amine complex (Am.BH 3 ); isolating said borazane and vacuum drying same; said temperature θ 1 being no lower than the melting temperature of said borane-amine complex (Am.BH 3 ). |
| priorityDate | 2014-05-23-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
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