Predicate |
Object |
assignee |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_077f0cd6000d9ec9f2c7d78df4ce23ff |
classificationCPCInventive |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C249-02 |
classificationIPCInventive |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C251-30 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C249-02 |
filingDate |
2013-03-05-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_f4b5bfc079ad1ac8b589145f1c8836b6 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_87d99c778011dbe5a2508ddb977a3a46 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_4f7966799ef53613b836873e184f939a http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_81bf4a705ab3cd48966385ea4d8f918e http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_bdce7f8753186d382ab509e4c39ef526 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_a978b58bd80e668a8cd0b8bd4facbcfe http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_256c729805b598fbaeb4143c260794a7 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_a9ee680178ad24d564fa204f34ee4b3b http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_4d885bbacaeb0546eebce0f708c48753 |
publicationDate |
2014-07-24-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber |
WO-2014110696-A1 |
titleOfInvention |
Process for preparing solid (chlorine methylene) dimethyl ammonium chloride |
abstract |
A method for preparing solid (chlorine methylene) dimethyl ammonium chloride. The method comprises: carrying out acylating chlorination reaction on raw materials of phthalic anhydride and thionyl chloride to obtain o-phthaloyl chloride; o-phthaloyl chloride reacting with N,N-dimethylformamide to obtain (chlorine methylene) dimethyl ammonium chloride and phthalic anhydride; dissolving the generated phthalic anhydride in excessive N,N-dimethylformamide; and obtaining solid (chlorine methylene) dimethyl ammonium chloride through solid-liquid separation. The method discharges sulfur dioxide through the first step of reaction, so that sulfur dioxide does not need to be forcedly removed in a high vacuum condition, thereby making the reaction condition mild and the implementation easy. |
priorityDate |
2013-01-18-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type |
http://data.epo.org/linked-data/def/patent/Publication |