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inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_3ce44791ee849482cb0b586a33254b6f
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publicationDate 2012-01-05-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber WO-2012002189-A1
titleOfInvention Method for producing valsartan
abstract Disclosed is a method for producing valsartan having a valsartan enantiomer content of 0.25% or less and an organic solvent content of 1000 ppm or less, comprising drying crude valsartan having a valsartan enantiomer content of 0.20% or less and an organic solvent content of 3000-25000 ppm inclusive at a temperature of 50-65ºC. The crude valsartan is obtained by, for example, drying a wet substance of valsartan having a valsartan enantiomer content of 0.20% or less and an organic solvent content of 150000-600000 ppm inclusive obtained by depositing synthetically obtained valsartan in an organic solvent and separating the deposited crystals of valsartan at a temperature lower than 50ºC.
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