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filingDate 2007-12-27-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_0ce540953fb8d20843356687a2eee563
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publicationDate 2008-07-03-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber WO-2008078340-A1
titleOfInvention Process for the separation of 4-bromomethyl-2'-substituted biphenyls from 4,4,-dibromomethyl-2'-substituted biphenyls
abstract Disclosed herein is process for the separation of 4-bromomethyl-2'-substituted biphenyls of Formula (II) from 4,4-dibromomethyl-2'-substituted biphenyls of Formula (III) and 4-methyl-2'-substituted biphenyl of Formula (I) by stirring a crude reaction mixture comprising compounds of Formula (I), (II) and (III) in suitable organic solvents at a temperature above 50°C; and gradually cooling the reaction mixture below 20°C to obtain pure crystals of Formula (II) with purity of more than 97%.
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