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filingDate 2006-10-16-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 2007-07-19-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber WO-2007080681-A1
titleOfInvention Process for producing crosslinked fluororubber
abstract [PROBLEMS] To provide a process for producing a polyol-crosslinked fluororubber which can realize low-tack properties and has a highly enhanced rubber hardness. [MEANS FOR SOLVING PROBLEMS] The process is characterized by subjecting a fluororubber composition which comprises a polyol-crosslinkable fluororubber, a crosslinking accelerator comprising a quaternary phosphonium salt or a quaternary ammonium salt, and a polyol-type crosslinking agent and in which the weight ratio of the crosslinking accelerator to the polyol-type crosslinking agent, X (crosslinking accelerator/polyol-type crosslinking agent), is 0.90-3.00 in the case of the quaternary phosphonium salt and is 0.4-0.6 in the case of the quaternary ammonium salt to thermal vulcanization with pressing to mold a vulcanizate, subsequently applying a treating liquid obtained by dissolving the polyol-type crosslinking agent and the crosslinking accelerator in a solvent to the surface of the vulcanizate, and then heating the coated vulcanizate at 200-300°C for 1-20 hours.
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