http://rdf.ncbi.nlm.nih.gov/pubchem/patent/WO-2006103693-A1

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filingDate 2005-11-29-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 2006-10-05-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber WO-2006103693-A1
titleOfInvention A process for the preparation of p-toluic acid by liquid phase oxidation of p-xylene in water
abstract The present invention provides a process for the preparation of p-toluic acid by liquid phase oxidation of p-xylene using oxygen or air as oxidant in the presence of p-toluic acid, water as solvent and cobalt salt or its combinations with salts of Ce, Mn as catalyst. Oxidation is carried out at 130-190°C and pressure sufficient to keep water in liquid state. Oxidation step is followed by filteration to obtain p-toluic acid as major product. Unreacted p-xylene is recovered and recycled and the catalyst is recovered from aqueous phase and is recycled.
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