| abstract |
A method of preparing a poly(arylene ether)includes oxidatively polymerizing a monohydric phenol in solution, concentrating the solution by removing a portion of the solvent to form a concentrated solution having a cloud point, Tcloud, and combining the concentrated solution with an anti-solvent to precipitate the poly(arylene ether), wherein the concentrated solution has a temperature of at least about (Tcloud-10 °C) imme diately before it is combined with the anti-solvent. The method reduces the formation of undesirably fine particles in the product poly(arylene ether). |