Predicate |
Object |
assignee |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_78720ff42af6c1ba6c5d3fc2ed72f2d6 http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_8339f73f47970072fe8cc5ea95ceeb69 http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_b2f986a5709f3df33b9c5b875328a3f0 http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_9b1892ecb6454477a5fdbbc6ffba8fae |
classificationCPCInventive |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C67-08 |
classificationIPCInventive |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C67-08 |
filingDate |
2000-10-26-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_09f38e368887ee782af219aaff2d3618 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_622de71c0d06eaa1d446f95e432d080a http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_a039038d808fe50674590d8918d1057a |
publicationDate |
2001-05-03-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber |
WO-0130299-A2 |
titleOfInvention |
Method of synthesizing alkyl gallates |
abstract |
A method for synthesizing alkyl gallates. Gallic acid and an alkyl alcohol of the order of the desired gallate are heated in a reaction vessel in the presence of a catalyst such as sulfuric acid or para-toluene sulfonic acid. Water is generated, forming an azeotrope with the alkyl alcohol. Distillation or Soxhlet extraction using a drying agent removes the formed water. Upon completion of the reaction, the reaction mixture is added while stirring to an alkane solvent and cooled to produce crystals of the desired alkyl gallate. The crystals may be further recrystallized and washed to improve their purity. |
isCitedBy |
http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-107488111-B http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-114807920-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/WO-0149248-A3 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-102351705-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-111807962-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-107488111-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/EP-1604660-A1 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-105111073-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/EP-1604660-A4 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-111747848-B http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-111747848-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-104086416-A |
priorityDate |
1999-10-27-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type |
http://data.epo.org/linked-data/def/patent/Publication |