Predicate |
Object |
assignee |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_c85d78c6a4459b5dbbc49c82a4c5c107 http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_fb78b459e21bb4fd52850a12cab27387 |
classificationCPCAdditional |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/Y02P20-10 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C02F2103-38 |
classificationCPCInventive |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C69-54 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C67-40 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C67-39 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C02F1-008 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C02F1-04 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/B01D3-4205 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C67-54 |
classificationIPCAdditional |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C02F103-38 |
classificationIPCInventive |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C02F1-04 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C67-40 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C67-54 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/B01D3-42 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C67-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C02F1-00 |
filingDate |
2015-10-02-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate |
2018-05-08-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_24b492d3ca95f7fb0edf571478665b8e http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_881d22e1829a68ffc05927bb0fd9a12c http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_de7ce6ed1be5d371030624e3e5c0a814 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_f7de3dd9321d9753af0b0f1e88f528e5 |
publicationDate |
2018-05-08-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber |
US-9963419-B2 |
titleOfInvention |
Process for in situ water removal from an oxidative esterification reaction using a coupled reactor-distillation system |
abstract |
A process for removing water from an oxidative esterification reactor includes (a) conducting an oxidative esterification reaction in a reactor; (b) removing a crude product stream from the reactor; (c) passing a first portion of the crude product stream directly to a product recovery zone; (d) introducing a second portion of the crude product stream to a distillation column to generate a column overheads stream and a column bottoms stream; (e) passing at least a portion of the columns bottoms stream to the product recovery zone; and (f) recycling a recycle stream comprising at least a portion of the overheads stream to the reactor; wherein the recycle stream contains less than 1 weight percent (wt %) water based on the total weight of the recycle stream, wherein the weight ratio of the first portion to the second portion is at least 1:10, and wherein the amount of the recycle stream recycled to the reactor is such that the reactor contains less than or equal to 2.5 wt % water, based on the weight of the reactor contents. |
priorityDate |
2014-10-31-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type |
http://data.epo.org/linked-data/def/patent/Publication |