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publicationDate 2018-02-27-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-9902700-B2
titleOfInvention Method and system for preparing caprolactam
abstract The present disclosure provides a method for preparing a caprolactam and the method includes steps of subjecting cyclohexanone oxime and sulfuric acid to a Beckmann rearrangement reaction to obtain a rearrangement mixture; neutralizing the rearrangement mixture and extracting the neutralized rearrangement mixture using an organic solvent sequentially; and subjecting the extracted organic solution to a hydrogenation reaction so as to simplify the process to produce a high quality caprolactam.
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