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filingDate 2010-02-15-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2016-01-12-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_d02991b7386133bd2f1a719565d49a28
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publicationDate 2016-01-12-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-9234113-B2
titleOfInvention Dispersion of particles of rutile titanium oxide, process for producing the same, and use of the same
abstract The invention provides a dispersion of particles of rutile titanium oxide wherein the particles of rutile titanium oxide have a D50 in a range of 1 to 15 nm and a D90 of 40 nm or less in particle size distribution as determined by a dynamic light scattering method; a specific surface area in a range of 120 to 180 m 2 /g as determined by a BET method; and a rate of weight loss of 5% or less as obtained by heating the particles of rutile titanium oxide from 105° C. to 900° C. n Such a dispersion of particles of rutile titanium oxide is obtained by a process according to the invention, which comprises: a first step in which an aqueous titanium tetrachloride solution is heated and hydrolyzed to obtain a slurry containing the precipitated particles of rutile titanium oxide; a second step in which the slurry obtained in the first step is filtered and washed with water to remove water-soluble salts dissolved therein from the slurry; a third step in which the slurry obtained in the second step is subjected to a hydrothermal reaction in the presence of an organic acid; a fourth step in which the slurry obtained in the third step is filtered and washed with water; a fifth step in which an acid is added to the slurry obtained in the fourth step, and the resulting mixture is subjected to a wet dispersion treatment, thereby obtaining a dispersion; and a sixth step in which excess acid and water-soluble salts are removed from the dispersion obtained in the fifth step.
priorityDate 2009-02-19-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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