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filingDate 2011-06-08-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 2015-05-19-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-9035108-B2
titleOfInvention Method for preparing chlorohydrins composition and method for preparing epichlorohydrin using chlorohydrins composition prepared thereby
abstract Provided are a method of preparing a chlorohydrin composition and a method of preparing epichlorohydrin by using a chlorohydrin composition prepared by using the method. The method of preparing chlorohydrins in which polyhydroxy aliphatic hydrocarbon is reacted with a chlorination agent in the presence of a catalyst includes performing at least one combination of a series of unit operations comprising a first reaction step, a water removal step, and a second reaction step in this stated order, wherein the method further includes mixing a chlorohydrin concentrate obtained by purifying the reaction mixture discharged from the final reaction step from among the reaction steps and a water-rich layer discharged from the water-removal step and diluting the mixture with water. The method of preparing epichlorohydrin includes contacting the chlorohydrin composition prepared by using the method of preparing a chlorohydrin composition with an alkaline agent.
priorityDate 2010-06-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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