http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-9006476-B2

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filingDate 2010-10-29-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2015-04-14-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_c4b9a2bc6b269c437361609a4a82caec
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publicationDate 2015-04-14-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-9006476-B2
titleOfInvention Process for the production of high-purity dimethyl carbonate
abstract A process for producing a high-purity dimethyl carbonate, which includes: (I) cooling a commercial grade dimethyl carbonate containing 1 ppm or more of chlorine to a temperature from +6° C. to −5° C. at a rate from 0.5-2° C./hour, to obtain a first solid dimethyl carbonate; (II) heating the first solid dimethyl carbonate to a temperature from −5° C. to +6° C. at a rate of 1-5° C./hour, to obtain a mixture comprising a second solid dimethyl carbonate and a predetermined amount of a first liquid dimethyl carbonate; (III) separating the first liquid dimethyl carbonate from the mixture, to obtain the second solid dimethyl carbonate; (IV) heating the second solid dimethyl carbonate to a temperature from 20° C. to 40° C., to obtain a second liquid dimethyl carbonate, wherein the second liquid dimethyl carbonate has a purity degree higher than 99.99% and a chlorine content lower than or equal to 1 ppm.
priorityDate 2009-11-04-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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Total number of triples: 28.