Predicate |
Object |
assignee |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_07c9542186133097bd6bbb7d92393090 |
classificationCPCAdditional |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07B2200-13 |
classificationCPCInventive |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C401-00 |
classificationIPCInventive |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C401-00 |
filingDate |
2013-03-14-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate |
2015-01-27-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_214f00a70b0c27e7ccb07906cd20d5f2 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_4c281f415e8eca6ccd916d8a7744d004 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_9e32c7cd7ab95eb4f3df6f918a37ecd0 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_70ac0a37ab754ca4f17e77681d361e39 |
publicationDate |
2015-01-27-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber |
US-8940916-B2 |
titleOfInvention |
Crystallization of (20R)-2-methylene-19-nor-24-difluoro-1α,25-dihydroxyvitamin D3 |
abstract |
Disclosed are methods of purifying the compound (20R)-2-methylene-19-nor-24-difluoro-1α,25-dihydroxyvitamin D 3 to obtain the compound in crystalline form. The methods typically include the steps of dissolving a product containing the compound in a solvent comprising hexane and 2-propanol, cooling the solvent and dissolved product below ambient temperature for a sufficient amount of time to form a precipitate of crystals, and recovering the crystals. |
isCitedBy |
http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-11697635-B2 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/WO-2019079279-A1 |
priorityDate |
2012-05-30-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type |
http://data.epo.org/linked-data/def/patent/Publication |