http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-8772537-B2

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assignee http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_24aca9ded2638ea793d05360dde7a4a0
http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_9748af4cd68faaa7866c392502a13e49
classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C309-00
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C315-02
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C381-04
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C381-02
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C309-00
filingDate 2011-07-22-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2014-07-08-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_b08340c18a76b7561abb1260a6ea9697
publicationDate 2014-07-08-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-8772537-B2
titleOfInvention Process for producing aminoalkylthiosulfuric acid compound
abstract An aminoalkylthiosulfuric acid compound represented by formula (1): n nis produced. In step (A1), a hydrochloride of a chloroalkylamine compound represented by formula (2):n n nis reacted with an alkali metal salt of thiosulfuric acid in the presence of 2 to 6 parts by weight of water with respect to 1 part by weight of the hydrochloride between 50° C. and 100° C. R 1 and R 2 each represents a hydrogen atom and the like, and n represents an integer of 2 to 9. In step (B1), a mixture of a solid containing the aminoalkylthiosulfuric acid compound and a liquid containing an alkali metal chloride is obtained by adjusting the temperature of the mixture of step (A1) to between −15° C. and 50° C. In step (C1), the aminoalkylthiosulfuric acid compound is obtained as solid by separating the solid containing the aminoalkylthiosulfuric acid compound and the liquid containing the alkali metal chloride from the mixture of (B1).
priorityDate 2010-07-28-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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