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filingDate 2009-11-23-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_55e651b088a0995415a162f1668062c2
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publicationDate 2012-11-13-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-8309361-B2
titleOfInvention Method for quantification of analytes in a titanium, tin or silicon tetrachloride sample
abstract This disclosure relates to a method for detecting at least one analyte in a tetrachloride sample comprising titanium, tin or silicon tetrachloride; comprising,n (a) adding a mixture of water and acid, typically hydrochloric acid, to the sample under conditions effective for forming an aqueous solution of the sample; (b) introducing the aqueous solution of the sample into an inductively coupled mass spectrometer having a cell selected from the group of a reactive cell and a collision cell or both and producing an analyte ion comprising an interfering species; (c) contacting the analyte ion with a gas to produce a product which is substantially free from the interfering species; and (d) detecting and measuring at least one signal from the analyte in the solution. This disclosure further relates to a method for making an aqueous titanium, tin or silicon tetrachloride sample suitable for analysis in using inductively coupled plasma mass spectroscopy.
priorityDate 2006-06-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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