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filingDate 2009-06-23-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2010-04-06-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 2010-04-06-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-7691288-B2
titleOfInvention Thick film getter paste compositions with pre-hydrated desiccant for use in atmosphere control
abstract The invention is directed to a process for making screen-printable getter composition comprising: (a) glass frit; and (b) pre-hydrated desiccant material; dispersed in (c) organic medium. The present invention further relates to a getter composition utilizing low-softening temperature glasses comprising, based on weight %, 1-50% SiO 2 , 0-80% B 2 O 3 , 0-90% Bi 2 O 3 , 0-90% PbO, 0-90% P 2 O 5 , 0-60% Li 2 O, 0-30% Al 2 O 3 , 0-10% K 2 O, 0-10% Na 2 O, and 0-30% MO where M is selected from Ba, Sr, Ca, Zn, Cu, Mg and mixtures thereof. The glasses described herein may contain several other oxide constituents that can substitute glass network-forming elements or modify glass structure. n The desiccant material is pre-hydrated to reach its saturation level of moisture absorption. The process of pre-hydration can be done by exposing the desiccant in a normal temperature/humidity environment of for example, 25° C. and 50-60% RH. For 24 to 48 hours or up to the time when weight gain (due to moisture absorption) stops increasing. An accelerated hydration process in a chamber with higher than normal humidity level (i.e. 50% Relative Humidity) is also applicable to shorten the time of exposure to fully hydrate the desiccant material.
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