http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-7557217-B2
Outgoing Links
Predicate | Object |
---|---|
assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_baee372c55802742f9582e25c15ff11a |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D401-12 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D401-12 |
filingDate | 2005-06-29-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2009-07-07-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_9f177abffc3714f519484d0cdd3501cb |
publicationDate | 2009-07-07-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | US-7557217-B2 |
titleOfInvention | Process for production of benzimidazole derivative salt precipitate |
abstract | The present invention provides a process for the production of a 2-[{4-(3-methoxypropoxy)-3-methylpyridin-2-yl}methylsulfinyl]-1 H-benzimidazole alkali metal salt (1), which is a drug or an intermediate for the production of a drug, the process not requiring large-scale equipment and being excellent in terms of workability, operability and energy conservation. According to the present invention, there is disclosed a process for the production of a salt precipitate represented by formula (1) n n(wherein B represents an alkali metal ion), the process comprising the steps of:n dissolving the compound represented by formula (2) n nin a first organic solvent and adding an alkali metal hydroxide, or dissolving the alkali metal hydroxide in the first organic solvent and adding the compound represented by formula (2); andn further adding a second organic solvent to a reaction mixture obtained. |
isCitedBy | http://rdf.ncbi.nlm.nih.gov/pubchem/patent/WO-2022148868-A1 |
priorityDate | 2004-06-30-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 74.