http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-7446221-B1

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filingDate 2007-06-05-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2008-11-04-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_2f6d8f5d5f5a85bb09c3e35eb9a3ff84
publicationDate 2008-11-04-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-7446221-B1
titleOfInvention Process for making tricyclodecenyl esters
abstract A practical, economical process for making tricyclodecenyl esters is disclosed. After reacting a lower carboxylic acid and a dicyclopentadiene in the presence of triflic acid to form the ester, the reaction mixture is distilled in the presence of a base to isolate a fragrance-quality tricyclodecenyl ester. Adding enough base to neutralize the triflic acid enables a distillation-only purification, facilitates starting material recovery, and avoids drawbacks of a basic workup.
priorityDate 2007-06-05-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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