http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-6479657-B1

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publicationDate 2002-11-12-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-6479657-B1
titleOfInvention Crystalline 1-kestose and process for preparing the same
abstract A process for producing crystal 1-kestose wherein granular crystal 1-kestose in the form of large crystals can be produced at a high yield is disclosed. A highly pure solution of 1-kestose is concentrated to a Brix of 75 or higher; either seed crystals are added, or the solution is vacuum-concentrated to generate microcrystals for use as nuclei; then, a crystal growing step by vacuum-concentration and a microcrystal dissolving step for redissolving microcrystals which have formed in the concentrate are repeated at least twice each. Alternatively, a highly pure solution of 1-kestose is concentrated to a Brix of 80 or higher; either seed crystals are added, or the solution is allowed to initiate crystallization; after crystals are allowed to grow, a cooling step where the temperature is lowered by 5° C. to 20° C. from the previous step and a crystal growing step where the concentrate is maintained at the temperature to allow the crystals to grow are repeated at least twice each. Also, an enzyme for producing 1-kestose efficiently from sucrose is disclosed.
isCitedBy http://rdf.ncbi.nlm.nih.gov/pubchem/patent/KR-20210052100-A
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http://rdf.ncbi.nlm.nih.gov/pubchem/patent/WO-2014044230-A1
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