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publicationNumber US-6413378-B1
titleOfInvention Apparatus for separation and purification of saturated hydrocarbon and method for separation and purification
abstract An extractive distillation tower 4 supplied with a feedstock containing butadiene and a solvent and for distilling the feedstock to separate and purify the butadiene. The tower 4 includes sensors 32, 34 for detecting concentrations of specific impurities other than butadiene; a sensor for detecting a concentration of the butadiene; a sensor 30 for detecting a differential pressure between the top and bottom of the tower 4; a valve 48 for controlling the flow rate of part of fluid taken out from a bottom of the tower 4 and returned to the tower 4; a valve 23 for controlling a ratio of a solvent fed to the tower 4; a reflux ratio valve 28 for controlling the flow rate of part of remaining component of the feedstock taken out from a top of the tower 4 and refluxed; a heater 36 for controlling a bottom temperature of the tower 4; and a predictive control 60 for calculating forecasted values of the concentrations of the specific impurity and the butadiene after a time based on these sensors and controlling the system based on the forecasted values.
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