Predicate |
Object |
assignee |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_7ef01e33058cf740cf2197991be97af1 |
classificationCPCInventive |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07F9-065 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07F9-02 |
classificationIPCInventive |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07F9-06 |
filingDate |
1998-12-01-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate |
2000-07-18-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_b8ad2d32bbeb7aad6befd4febf2cb8c5 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_4698eb12b6f06b249d96ff7975240994 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_273b380a20cf5946d33ddbf5ae0b0c66 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_b6adddf7ee843f5036540e47baf3d9e1 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_27c41e2c50a8b7fb5aa71f657a344434 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_b49d67b9ce03b44eaab8d86b0b7a129e http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_d19e19635ab9dd6c10aa7fa81c222a09 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_e793a421cedb0d620075aa2e37a3f9cb |
publicationDate |
2000-07-18-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber |
US-6090980-A |
titleOfInvention |
Preparation process of iminotris ( Dimethylamino) phosphorane |
abstract |
A process is provided for preparing iminotris(dimethylamino)phosphorane at high purity and high yield from aminotris(dimethylamino)phosphonium chloride. Aminotris(dimethylamino)phosphonium chloride is first reacted with an aqueous solution of the hydroxide of an alkali metal or alkaline earth metal in the presence of a solvent in which the chloride and hydroxide of the alkali metal or alkaline earth metal are sparingly soluble, whereby iminotris(dimethylamino)phosphorane is formed. After water is dissolved off at a temperature of 70° C. or lower from the reaction mixture, solids are removed from the thus-concentrated reaction mixture by solid-liquid separation. The resultant mother liquor is then distilled to obtain iminotris(dimethylamino)phosphorane. |
isCitedBy |
http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-10689475-B2 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-2015183918-A1 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-6444847-B2 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-10280246-B2 |
priorityDate |
1997-12-04-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type |
http://data.epo.org/linked-data/def/patent/Publication |