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filingDate 1997-05-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2000-06-06-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_8ffb6d9a3a09a80ab0e0604d8e53721d
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publicationDate 2000-06-06-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-6071485-A
titleOfInvention Process for the preparation of a micro-meso porous material with a high surface area and controlled distribution of the porosity
abstract The present invention relates to a process for the preparation of a micro-meso porous material which comprises: n a) preparing a mixture starting from a tetraalkylorthosilicate, a C 3 -C 6 alkyl alcohol or dialcohol, a tetraalkylammonium hydroxide having the formula R 1 (R 2 ) 3 N--OH wherein R 1 is a C 3 -C 7 alkyl and R 2 is a C 1 or C 3 -C 7 alkyl, optionally in the presence of one or more metal compounds, in which the molar ratios are within the following ranges: n alcohol/SiO 2 <or equal to 20; n R 1 (R 2 ) 3 N--OH/SiO 2 =0.05-0.4; n H 2 O/SiO 2 =1-40; n metal oxides/SiO 2 =0-0.02; n b) subjecting this mixture to hydrolysis and subsequent gelation at a temperature of between 20° C. and a temperature close to the boiling point of the alcohol or mixture of alcohols present; n c) subjecting the gel obtained to drying and calcination.
priorityDate 1996-06-13-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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