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publicationDate 2000-05-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-6057472-A
titleOfInvention Highly pure alkyl 2-cyanoacrylates
abstract A process for the preparation of a highly pure alkyl 2-cyanoacrylate, wherein alkyl has 1-10 C atoms, characterized in that a) formaldehyde is reacted with an alkyl cyanoacetate ester by means of a catalyst in a solvent mixture selected from the group comprising ethylacetate, diglyme, dichloroethane and benzene, yielding an oligo-(alkyl 2-cyanoacrylate); b) the product of (a) is separated in the form of a solid; c) the product of (b) is depolymerized under sulfur dioxide atmosphere free from other polymerization inhibitors to yield an alkyl 2-cyanoacrylate with a purity of 98-100%
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