http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-5824804-A
Outgoing Links
Predicate | Object |
---|---|
assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_e83d93ed02bbd6159e99b5a7796e3686 |
classificationCPCAdditional | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/Y02P20-582 |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D209-48 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D209-48 |
filingDate | 1997-09-12-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 1998-10-20-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_1e9f66488273aea8157f098111242fbc http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_4b30567ce9a7cf9c2ee434819f82d6d3 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_175af9268bc2013a295858246dedc181 |
publicationDate | 1998-10-20-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | US-5824804-A |
titleOfInvention | Method for the preparation of a N-alkoxy-(tetra-or hexahydro)-phthalimide and method for the preparation of a N-alkoxyamine |
abstract | Method for the preparation of N-alkoxy-(tetra- or hexahydro)-phthalimide according to formula I ##STR1## R 1 being methyl or ethyl and R 2 and R 3 being each independently of one another hydrogen or alkyl with 1-4 C atoms or R 2 and R 3 together with the carbon atom to which they are bonded forming a ring with 5 or 6 C atoms, wherein the salt of the corresponding N-hydroxy-(tetrahydro- or hexahydro)-phthalimide according to formula II: ##STR2## with R 2 and R 3 as defined above and M being an alkali metal, is brought into contact with R 1 Cl as alkylating agent, wherein R 1 has the aforementioned meaning. n The N-alkoxy-(tetra- or hexahydro)-phthalimide can afterwards be converted with the aid of hydroxylamine sulphate into the corresponding alkoxyamine after which the alkoxyamine obtained can be isolated. In this manner a simple and commercially attractive process for the preparation of O-(m)ethylhydroxylamine can be implemented. |
priorityDate | 1995-03-24-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 74.