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filingDate 1997-07-01-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 1998-06-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 1998-06-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-5773673-A
titleOfInvention Method of making chlorinated hydrocarbons
abstract Disclosed is a method of making chlorinated hydrocarbons. A mixture is prepared of a hydrocarbon or partially chlorinated hydrocarbon from C 18 to C 30 and either benzotrifluoride or parachlorobenzotrifluoride in an amount sufficient to liquefy the mixture at the chlorination temperature. The mixture is heated to a temperature of about 50° to 100° C. and sufficient chlorine gas is passed therethrough in the presence of UV light to form a chlorinated hydrocarbon that is about 60 to about 80 wt. % chlorine. One part by weight of the composition is added to at least two parts by weight per part of a C 1 to C 6 monohydric alcohol, which results in the precipitation of the chlorinated hydrocarbon. The precipitated chlorinated hydrocarbon can be removed from the composition by, for example, filtration.
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