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publicationDate 1997-12-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-5696283-A
titleOfInvention Preparation of methyl isoproylideneaminooxyacetoxyacetate
abstract Process for preparing methyl isopropylideneaminooxyacetoxyacetate I ##STR1## by reacting in an integrated process, a) acetone with hydroxylammonium sulfate and sodium hydroxide solution to give acetone oxime, the reaction being performed in the presence of toluene and/or the acetone oxime being extracted from the reaction mixture with toluene, n b) treating the toluene solution thus obtained with sodium hydroxide solution and removing water, n c) exchanging toluene for a dipolar aprotic solvent by distillation, n d) reacting the crystal mash thus obtained with the sodium salt of chloroacetic acid to give the sodium salt of isopropylideneaminooxyacetic acid and then treating the reaction mixture with methyl chloroacetate and n e) isolating the methyl isopropylideneaminooxyacetoxyacetate formed in d).
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