Predicate |
Object |
assignee |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_c7ad58d3c0b071069a8ee0cb8c8ba2e8 |
classificationCPCInventive |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C313-14 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C319-06 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C319-24 |
classificationIPCInventive |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C319-24 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C323-09 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C313-14 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C319-06 |
filingDate |
1995-06-01-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate |
1997-08-19-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_7cec753d2b84675f66484c8a6eb60820 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_f8a248cc061a61d208acd878c387f0cd http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_7e58604471531fe371a930b7a306e08d http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_f4c32fc73bd226e1d683986816e57645 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_5204e76051b57e501293b04c5b01677a |
publicationDate |
1997-08-19-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber |
US-5659088-A |
titleOfInvention |
Process for the preparation of 4-fluorothiophenol |
abstract |
4-Fluorothiophenol is obtained in outstanding purifies and yields if 4-fluorobenzenesulphonyl chloride is reacted with sodium hydrogen sulphite solution to give a solution of sodium 4-fluorobenzenesulphinate, this solution is reduced with sulphur dioxide to give 4,4'-difluorodiphenyl disulphide and finally this is reacted with sodium borohydride in a water-miscible inert organic solvent to give 4-fluorothiophenol (sodium salt). Free 4-fluorothiophenol can be isolated from the sodium salt solution by acidification. |
isCitedBy |
http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-6271415-B1 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-109574881-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-6500988-B1 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/WO-2007066845-A1 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-102875431-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/WO-2007066844-A1 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-111187188-A |
priorityDate |
1994-06-15-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type |
http://data.epo.org/linked-data/def/patent/Publication |