http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-5545771-A

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filingDate 1993-03-12-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 1996-08-13-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_d7728be5f5d6d072b69b5e7261e93b02
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publicationDate 1996-08-13-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-5545771-A
titleOfInvention Process for preparation of gem-difluoroalkanes
abstract A process for preparation of a gem-difluoroalkane is provided which comprises n (A) a step to add a fluorinated alkane having a boiling point of -30° to 30° to a crude alkyne having 3 or 4 carbon atoms containing a polymerizable olefin as an impurity, and distill the mixture to remove the polymerizable olefin, n (B) a step to react hydrogen fluoride with the fluorinated alkane and the alkyne having 3 or 4 carbon atoms obtained in the above step to synthesize the gem-difluoroalkane, and n (C) a step to distill the reaction solution of the above (B) to obtain the gem-difluoroalkane. n According to this process, gem-difluoroalkanes can be prepared more economically compared with usual processes.
priorityDate 1992-03-16-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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Total number of triples: 46.