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filingDate 1992-03-12-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 1994-02-22-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_0d039072ac42482eff25c5867f78d83a
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publicationDate 1994-02-22-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-5288881-A
titleOfInvention Continuous reduced pressure dimeric cyclic ester production
abstract An improved process for converting oligomers of alphahydroxycarboxylic acids, such as glycolic and lactic acid, to dimeric cyclic esters, such as glycolide and lactide. The continuous process is conducted at reduced pressures and depolymerizing temperatures in a heated columnar depolymerization zone, coupled with an essentially unheated receiver for unconverted oligomer. By feeding the oligomer to the upper end of the column while coordinating the feed rate with the depolymerization temperature such that a fraction of the oligomer is converted to a vapor product stream containing the cyclic ester and another fraction of the oligomer exits the column at its lower end and passes to the receiver vessel, the dimeric cyclic ester is produced at high production rates and the oligomer is subjected to minimal thermal stress.
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http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-5521278-A
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http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-6005067-A
priorityDate 1992-03-12-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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Total number of triples: 53.