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filingDate 1992-10-15-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 1994-01-04-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_dc9065fafec3a2df5d0b448e30beb9b4
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publicationDate 1994-01-04-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber US-5276200-A
titleOfInvention Method of preparing sodium formyl acetone and 4,4-dimethoxy-2-butanone
abstract The present invention provides a method of preparing sodium formyl acetone using acetone, methyl formate and sodium methoxide as raw materials. A mixture consisting of an acetone and a methyl formate is supplied to a methanol solution of sodium methoxide, or an acetone and a methyl formate are separately supplied simultaneously to the methanol solution of sodium methoxide. The resultant mixture is sufficiently stirred over a predetermined period of time so as to carry out the reaction to form sodium formyl acetone. Also provided is a method of preparing 4,4-dimethoxy-2-butanone. In this method, the reaction mixture obtained in the reaction to form sodium formyl acetone is directly charged into a reaction vessel simultaneously with sulfuric acid to neutralize and acetalize sodium formyl acetone contained in the reaction mixture so as to obtain 4,4-dimethoxy-2-butanone.
isCitedBy http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-102010311-A
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